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impinging on the sample is readily calculated from knowledge of the input polarizations, yet in the bulk of the material the light pattern will be redirected and repolarized on the basis of the detailed three-dimensional structure of the surface, refractive index, and birefringence. The optical erasure of an SRG, performed by homogenous irradiation, is also polarization-dependent (LagugneLabarthet et al., 2002; Jiang et al., 1998). Thus, the gratings possess a memory of the polarization state during inscription, encoded in the orientational distribution of chromophores at various grating positions. Typically, gratings inscribed with highly favorable polarization combinations will be optically erased more quickly. The s-polarization state, which produces poor gratings, is generally optimal for performing the erasure. These results are obviously related to the orientational distribution of chromophores after surface patterning and their subsequent interaction with the erasing polarization.

By this transformation, an important set of values, the power spectrum, )\2 (5.8.19)

is obtained. The analysis of the power spectrum, the aim of which is, for example, to determine the characteristic constants of the processes from which the noise stems will not be discussed here and the reader is recommended to inspect the relevant papers listed on page 384. The electrocrystallization on an identical metal substrate is the slowest process of this type. Faster processes which are also much more frequent, are connected with ubiquitous defects in the crystal lattice, in particular with the screw dislocations (Fig. 5.25). As a result of the helical structure of the defect, a monoatomic step originates from the point where the new dislocation line intersects the surface of the crystal face. It can be seen in Fig. 5.48 that the wedge-shaped step gradually fills up during electrocrystallization; after completion it slowly moves across the crystal face and winds up into a spiral. The resultant progressive spiral cannot disappear from the crystal surface and thus provides a sufficient number of growth

In a typical inscription experiment, a sinusoidally varying light pattern is generated at the sample surface. What results is a sinusoidal surface pro le: an SRG. This is the pattern most often reported in the literature, because it is conveniently generated (by intersecting two coherent beams) and easily monitored (by recording the diffraction intensity at a nonabsorbing wavelength, usually using a HeNe laser at 633 nm). However, it must be emphasized that the azo surface mass transport can produce arbitrary patterns. Essentially, the lm encodes the impinging light pattern as a topography pattern. Both the intensity

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Fig. 5.49 A microphotograph of low pyramid formation during electrocrystallization of Ag on a single crystal Ag surface. (By courtesy of E. Budevski)

and polarization of light are encoded What appears to be essential is a gradient in the intensity or polarization of the incident light eld For instance, a single focused gaussian laser spot will lead to a localized depression and a gaussian line will lead to an elongated trench (Bian et al, 1998) In principle, any arbitrary pattern could be generated through an appropriate mask, interference/holographic setup, or scanning of a laser spot (Natansohn and Rochon, 2002) Concomitant with the inscription of a surface relief is a photoorientation of the azo chromophores, which depends on the polarization of the incident beam(s) The orientation of chromophores in SRG experiments has been measured using polarized Raman confocal microspectrometry (Lagugne-Labarthet et al, 2004; Labarthet et al, 2004, 2000) The strong surface orientation is con rmed by photoelectron spectroscopy (Henneberg et al, 2004).