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explicitly included in the model, as it serves to align dipoles and thus enhance the mean- eld force. Because of this, even pure polarization patterns lead to gratings in this model. This mechanism appeals to the unique properties of azobenzenes only to explain the photoorientation of dipoles. If this mechanism were general, one would expect it to operate on nonisomerizing dipoles that had been aligned by other means, which has not yet been observed.

Fig. 5.55 Different paths of anodic oxidation dependent on electrolyte composition. (According to L. E. Eberson and N. L. Weinberg)

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A mechanism involving spatial variation of the permittivity, e, has been suggested by Baldus and Zilker (2001). This model assumes that a spatial modulation of the refractive index, hence permittivity, is induced in the lm. This is certainly reasonable, given the well-known photoorientation and birefringence gratings in azo systems. A force is then exerted between the optical electric eld and the gradient in permittivity. Speci cally, the force is proportional to the intensity of the electric eld in the mass transport direction and to the gradient of the permittivity: e0 ~ ~ f E 2 re 2 4:6

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387 reduction of nitrobenzene, azoxybenzene and hydrazobenzene are produced as a result of interactions among the adsorbed intermediates. If azobenzene is reduced in acid medium to hydrazobenzene, then the product rearranges in a subsequent chemical reaction in solution to give benzidine. An example of dimerization of the intermediates of an electrode reaction is provided by the reduction of acrylonitrile in a sufficiently concentrated aqueous solution of tetraethylammonium p -toluene sulphonate at a mercury or lead electrode. The intermediate in the reaction is probably the dianion CH 2 =CHCN + 2 e ^ CH2 CHCN (5.9.4)

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which reacts in the vicinity of the electrode with another acrylonitrile molecule CH2 CHCN + CH 2 =CHCN-* NCCHCH2CH2CHCN (5.9.5) (-) (-) NCCHCH2CH2CHCN + 2H 2 O-^ NC(CH2)4CN + 2OH~ finally to form adiponitrile (an important material in the synthesis of Nylon 606). Carbonyl compounds are reduced to alcohols, hydrocarbons or pinacols (cf., for example, Eq. 5.1.8), where the result of the electrode process depends on the electrode potential. The electrocatalytic oxidation of methanol was discussed on page 364. The extensively studied oxidation of simple organic substances is markedly dependent on the type of crystal face of the electrode material, as indicated in Fig. 5.56 for the oxidation of formic acid at a platinum electrode. M. Faraday was the first to observe an electrocatalytic process, in 1834, when he discovered that a new compound, ethane, is formed in the electrolysis of alkali metal acetates (this is probably the first example of electrochemical synthesis). This process was later named the Kolbe reaction, as Kolbe discovered in 1849 that this is a general phenomenon for fatty acids (except for formic acid) and their salts at higher concentrations. If these electrolytes are electrolysed with a platinum or irridium anode, oxygen evolution ceases in the potential interval between +2.1 and +2.2 V and a hydrocarbon is formed according to the equation 2 R C O O " ^ R2 + 2CO2 + 2e (5.9.6)

Mass is thus driven out of areas with a strong gradient in e, which generally moves material into the dark (consistent with the phase relationship in amorphous systems). Here again the mechanism appears general: any system with spatial variation of refractive index should be photopatternable, yet this is not observed. This model would appear to require that adequate photoorientation precede mass transport. Most experiments indicate, however, that both orientational and surface relief phenomena begin immediately and continue concurrently throughout inscription. This model was used to explain SRG formation in pulsed experiments (Baldus et al., 2001; Leopold et al., 2000), where thermal effects were suggested as giving rise to the spatial variation of permittivity, but the resulting force was essentially identical. However, conventional laser ablation appears to be a simpler explanation for those results (Yager and Barrett, 2004).

The principles of clustering came from the multiprocessing work that already had been done by companies like IBM and CDC. Computer clusters are loosely coupled multiprocessing implementations. Each computer in the cluster is a node with its own processor(s) (clusters can be created with multiprocessing nodes and often are), operating system, memory, and system storage. There may or may not be a shared storage pool; however, very few clusters today are implemented with shared data. Initially clusters were simply separate workstations on a network. However, with shrinking footprints and increased costs for space, often cluster nodes were rack-mounted, one on top of the other. Today blade servers enable clustering in even smaller footprints, as well as shared power and cooling. The first commodity clustering product in the open-systems market was ARCnet, developed and released by Datapoint in 1977. ARCnet wasn t successful in the market and clustering lay dormant until DEC released their

In addition to hydrocarbons, other products have also been found, especially in the reactions of the higher fatty acids. In steady state, the current density obeys the Tafel equation with a high value of constant 6 0.5. At a constant potential the current usually does not depend very much on the sort of acid. The fact that the evolution of oxygen ceases in the

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