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Fleischmann, M., and H. R. Thirsk, Electrocrystallization and metal deposition, AE, 3, 123 (1963). Froment, M. (Ed.), Passivity of Metals and Semiconductors, Elsevier, Amsterdam, 1983. Gilman, S., see page 368. Kokkinidis, G., Underpotential deposition and electrocatalysis, J. Electroanal. Chem., 201, 217 (1986). McCafferty, E., and R. J. Broid (Eds), Surfaces, Inhibition and Passivation, Ellis Horwood, Chichester, 1989. Pospisil, L., Random processes in electrochemistry, in J. Koryta et ai, Contemv poraneous Trends in Electrochemistry (in Czech), Academia, Prague, 1986, p. 14. Stefec, R., Corrosion Data from Polarization Measurements, Ellis Horwood, Chichester, 1990. Uhlig, H. H., Corrosion and Corrosion Control, John Wiley & Sons, New York, 1973. Vermilyea, D. A., Anodic films, AE, 3, 211 (1963). Vetter, K. J., see page 353. Young, L., Anodic Films, Academic Press, New York, 1961. 5.9 Organic Electrochemistry

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QuaggaJS, an advanced barcode - reader written in JavaScript
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chemistry is an ever-expanding research domain It is no surprise that the clean and unique azo photochemistry has been applied to switching biological systems (Willner and Rubin, 1996) One of the earliest investigations of azobenzene in a biological context involved embedding azobenzene molecules into a model membrane system (Balasubramanian et al, 1975) On isomerization, the lamellae were disrupted and rearranged, which also changed the enzymatic activity of membrane-bound proteins The catalytic activity of a cyclodextrin with a histidine and azobenzene pendant was photocontrollable because the trans version of the azo pendant can bind inside the cyclodextrin pocket, whereas the cis version liberated the catalytic site (Lee and Ueno, 2001) Photoregulation of polypeptide structure has been an active area of research (Ciardelli and Pieroni, 2001), with the azobenzenes making signi cant contributions Azo-modi ed poly (L-alanine) (Sisido et al, 1991a,b), poly(L-glutamic acid) (Houben et al.

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As this broad subject has been treated in a great many monographs and surveys and falls largely in the domain of organic chemistry, the treatment here will be confined to several examples. The tendency of an organic substance to undergo electrochemical reduction or oxidation depends on the presence of electrochemically active

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, 1983; Pieroni et al, 1980), and poly(L-lysine) (Malcolm and Pieroni, 1990), among others, have been prepared Depending on the system, photoisomerization may cause no change (Houben et al, 1983) or can induce a substantial conformational change, including transitions from ordered chiral helix to disordered achiral chain (Fissi et al, 1996; Yamamoto and Nishida, 1991; Montagnoli et al, 1983), changes in the a-helix content, or even reversible a-helix to b-sheet conversions (Fissi et al, 1987) Also, owing to the change in local electrostatic environment, the pKa of the polypeptides can be controlled in these systems Covalent attachment of azobenzene units to enzymes can modify protein activity by distorting the protein structure with isomerization This was used to control the enzyme activity of papain (Willner and Rubin, 1993; Willner et al, 1991a) and the catalytic ef ciency of lysozyme (Inada et al, 2005).

groups in the molecule, on the solvent, on the type of electrolyte and especially on the nature of the electrode. While oxidation processes at the mercury electrode are limited to hydroquinones and related substances, radical intermediates formed by cathodic reduction (e.g. in the potentiostatic double-pulse method) and some substances forming complexes with mercury, almost all organic substances can be oxidized under suitable conditions at a platinum electrode (e.g. saturated aliphatic hydrocarbons in quite concentrated solutions of sulphuric or phosphoric acid at elevated temperatures). The reduction of organic substances requires the presence of a jr-electron system, a suitable substituent (e.g. a halogen atom), an electron gap or an unpaired electron in the molecule. The electrode reaction of an organic substance that does not occur through electrocatalysis begins with the acceptance of a single electron (for reduction) or the loss of an electron (for oxidation). However, the substance need not react in the form predominating in solution, but, for example, in a protonated form. The radical formed can further accept or lose another electron or can react with the solvent, with the base electrolyte (this term is used here rather than the term 'indifferent' electrolyte) or with another molecule of the electroactive substance or a radical product. These processes include substitution, addition, elimination, or dimerization reactions. In the reactions of the intermediates in an anodic process, the reaction partner is usually nucleophilic in nature, while the intermediate in a cathodic process reacts with an electrophilic partner. According to G. J. Hoijtink, aromatic hydrocarbons are usually reduced in aprotic solvents in two steps:

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