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where T1 is the characteristic time of the decay process. For comparison, the photoisomerization behavior of a stable dispersion of the PEAPE colloids can be obtained in the same way. Both experimental data and tting curves are shown in Fig. 5.17. T1 obtained from the curve tting are 43.4 and 37.3 s for the hybrid colloids and PEAPE colloids, respectively. Comparing with the monocomponent PEAPE colloids, the trans-to-cis isomerization rate is far slower for the hybrid colloids. The hybrid colloids can show photoinduced deformation, and deformation ability is dependent on the percentage of the BP-AZ-CA component in the colloids. The experimental conditions for the sample preparation and light irradiation are the same as those mentioned earlier. The colloidal spheres were exposed to the spatially ltered and collimated laser beam incident perpendicularly on the substrate surfaces. The morphologies of colloidal spheres were observed by TEM before and after the laser irradiation. For comparison, the hybrid colloids and the monocomponent colloids were studied by the same light irradiation condition.

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Because of the electroosmotic flux, a cation-exchanger membrane is less resistant to cation flux than to anion flux. Some of the elements of thermodynamics of irreversible processes were described in Sections 2.1 and 2.3. Consider the system represented by n fluxes of thermodynamic quantities and n driving forces; it follows from Eqs (2.1.3) and (2.1.4) that \n{n +1) independent experiments are needed for determination of all phenomenological coefficients (e.g. by gradual elimination of all the driving forces except one, by gradual elimination of all the fluxes except one, etc.). Suitable selection of the driving forces restricted by relationship (2.3.4) leads to considerable simplification in the determination of the phenomenological coefficients and thus to a complete description of the transport process. The theory of transport in membranes is based on the thermodynamics of irreversible processes (Sections 2.1 and 2.3). If n species are involved in the transport, we have to consider n independent fluxes (including that of the solvent), each of them characterized by n phenomenological coefficients. Owing to the Onsager reciprocity relations, however, there are only n(n + l)/2 independent phenomenological coefficients, which can be determined by as many independent experiments. As usual in the theory of transport in electrolyte solutions, the driving forces are gradients of electrochemical potentials (in dilute solutions gradients of concentrations and of the electric potential can also be used). Consider the system shown in Fig. 6.3. The ion-exchanger membrane separates solutions of a single, completely dissociated, uni-univalent electrolyte. Two pistons can be employed to form a pressure difference between the two compartments. The two electrodes W^ and W2 are

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Fig. 6.3 A membrane system during flow of electric current. Ap p2 ~P\> Acs = cs(2) cs(l). S denotes the current source connected to an external source S to produce a flow of electric current through the membrane. Two usually identical reference electrodes are placed in the two compartments (e.g. two saturated calomel electrodes) and are used to measure the membrane potential. Since the ionic fluxes cannot be measured individually, it is preferable to introduce the salt flux, besides solvent flux and charge flux (current density). The driving forces would then be the gradients or differences of the chemical potentials in media with different salt concentrations and different pressures, multiplied by 1. These differences must be relatively small to remain within the framework of linear irreversible thermodynamics, so that RTAcs vsAp (6.2.13)

Figure 5.17. A plot of the relative absorbance (At /Aorigin) varying with the irradiation time and the tting curve for the dispersion containing PEAPE/BPAZ-CA (1:1, wt:wt) colloids, prepared by adding water into the THF-H2O solution. The data and tting curve for PEAPE colloidal dispersion are also given for comparison. Source: From Deng et al., 2007.

where cs is the salt concentration, cw is the solvent concentration, cs and cw are the average salt and solvent concentrations between the two compartments, respectively, vs and uw are the molar volumes of the salt and the solvent, respectively, and Ap is the pressure difference between the two compartments, t Even then, the formulation of the system of fluxes and driving forces is not yet satisfactory, because of the quantity Acw. Thus, a new definition of the fluxes will be introduced, i.e. the volume flux of the solution, defined by the equation

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