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The osmotic pressure of an electrolyte solution n can be considered as the ideal osmotic pressure JZ* decreased by the pressure jrel resulting from electric cohesion between ions. The work connected with a change in the concentration of the solution is n dV = n* dV JtcX dV. The electric part of this work is then jre, dV = dWeU and thus JZCX = (dWel/dV)Ttn. The osmotic coefficient (j> is given by the ratio jt/jt*, from which it follows that

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frozen in the process In this nucleation and gradual growth process, polymeric chains organize themselves from cores to shells in the hydrophobicity decrease order The self-assembling process is schematically illustrated in Fig 57 Because of this formation process, the colloidal spheres have cores formed from the most hydrophobic chains and coronas composed of the most hydrophilic chains The self-assembly mechanism is supported by the studies on the polymers given in Figs 51 and 52 as well as some others with similar structures The information about the growth process has been obtained from DLS measurements and in situ UV-vis spectroscopic study as mentioned earlier The structures formed in the suspensions at different aggregation stages can also be obtained by quenching the aggregates with excess water and characterized by transmission electron microscopy (TEM) after separation from the suspension.

(L3 34)

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as the ideal osmotic pressure is jt* = kNAT ch In order to obtain (dWJdV)T,n> Eq. (1.3.20) is differentiated, resulting in

The results also indicate that colloidal size increases with the increase in water content (Li et al, 2005a) The water content at which polymeric chains are completely involved in the aggregates can be obtained by using the parameters obtained for plotting, such as Fig 54 and the initial polymer concentration in THF solution (Li et al, 2006a; Zhang et al, 1997) The result shows that this water content is much higher than CWC, which is consistent with the gradual assembly scheme proposed earlier The aggregate collapse stage has been evidenced by the photoisomerization study aforementioned, which indicates the free-volume decrease during the process The average sizes of the colloidal spheres in the systems depend on the relative rates of the nucleation and gradual growth processes The in uence of the waterdropping rate can be explained by considering this factor.

Consider a dilute solution of a single electrolyte, so that cz = c + 4- c_, c + z + + c_z_=0 and /= 5Z + z_c. Comparison of Eq. (1.3.35) with Eq. (1.3.22) written for y and with Eq. (1.3.23) yields the limiting relationship

When the water addition rate is in a proper range, suf cient amount of nuclei can be formed in the initial stage The colloids with proper sizes can be obtained after the growth process and will be stable in the suspension because of the electrostatic repulsive force between the colloids, which can result from the overlap of the similar-charged electric double layers However, when the water addition rate is too slow, the colloids will become too large to be stably dispersed in the medium and will precipitate from the system..

More information about the following OASIS standards and activities can be found at http://www.oasis-open.org.

(1.3.36)